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Beilstein J. Org. Chem. 2011, 7, 802–807, doi:10.3762/bjoc.7.91
Graphical Abstract
Scheme 1: Au-catalyzed cyclization reactions of monoallylic diols.
Scheme 2: Reaction conditions for the preparation of 8.
Figure 1: QuadraPureTM MPA.
Figure 2: Quenching experiments using 9. = quenched after 1 min; = quenched after 3 min; = quenched after ...
Figure 3: Reaction progress in cis- and trans-diols. Conditions: 5 mol % Au[P(t-Bu)2(o-biphenyl)]SbF6, CH2Cl2...
Figure 4: Reaction progress in cis- and trans-methyl ethers. Conditions: 5 mol % Au[P(t-Bu)2(o-biphenyl)]SbF6...
Figure 5: A comparison of commonly used protecting groups. Conditions: 5 mol % Au[P(t-Bu)2(o-biphenyl)]SbF6, ...
Figure 6: Comparison of 1° and 2° allylic ethers. Conditions: 5 mol % Au[P(t-Bu)2(o-biphenyl)]SbF6, CH2Cl2, M...